000			03332cam a22003134a 4500
001			16489802
003			OSt
005			20210930190056.0
008			101005s2011 flua b 001 0 eng
010			_a 2010038460
020			_a9781439813126 (hardback)
040			_aDLC _cDLC _dDLC
042			_apcc
050	0	0	_aQD77 _b.L47 2011
082	0	0	_a543.028/4 _222
084			_aSCI013060 _2bisacsh
100	1		_aLerner, Leonid.
245	1	0	_aSmall-scale synthesis of laboratory reagents with reaction modeling / _cLeonid Lerner.
260			_aBoca Raton : _bCRC Press, _cc2011.
300			_axv, 217 p. : _bill. ; _c24 cm.
504			_aIncludes bibliographical references and index.
520			_a"The in-lab preparation of some chemical reagents provides a number of advantages over purchasing commercially-prepared samples. This volume contains a detailed description of methods for the rapid and reliable synthesis of many useful reagants that are otherwise difficult to obtain. It provides spectroscopic analyses of products, presents the thermodynamic/kinetic data of reactions, and offers a thorough analysis of the purity of the final products. Enhanced by useful diagrams and photographs, this text is a valuable reference for researchers in small or remote laboratories"-- _cProvided by publisher.
520			_a"When working in a small chemical laboratory attached to a non-chemistry specific project one is frequently asked to solve problems which occur in the main project. Usually one can think of several solutions and experimental testing is required to choose between the different approaches, or indeed to find an approach that works. These often require the use of small amounts of chemicals which the laboratory does not stock. Obtaining these chemicals from commercial suppliers in a suitable timeframe sometimes poses problems. This is particularly the case in isolated regions such as Australasia, when the supplier has no local stocks of hazardous substances and they have to be brought in from overseas, something which can introduce delays from several weeks to six months or more. Since there is no certainty that the substance whose acquisition is introducing the delay will form part of the ultimate solution, this delay is particularly objectionable. The primary aim of this book is therefore to provide reliable laboratory syntheses of the most common reagents whose acquisition can introduce delays due to their hazardous nature. It is apparent that there is little point in replacing delays in reagent purchase with uncertainties in their synthesis, hence the preparations presented in this book were chosen with the following criteria in mind: short duration, availability of apparatus, high yield, and high purity of the product. It was also considered necessary for the syntheses to be described in greater detail than is normally provided in the literature, since I have frequently found that omission of apparently small details can subsequently waste much time"-- _cProvided by publisher.
650		0	_aChemical tests and reagents _xSynthesis.
650		7	_aSCIENCE / Chemistry / Industrial & Technical _2bisacsh.
906			_a7 _bcbc _corignew _d1 _eecip _f20 _gy-gencatlg
942			_2lcc _cBK
999			_c265 _d265