MARC details
| 000 -LEADER |
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| fixed length control field |
03332cam a22003134a 4500 |
| 001 - CONTROL NUMBER |
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| control field |
16489802 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
OSt |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20210930190056.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
101005s2011 flua b 001 0 eng |
| 010 ## - LIBRARY OF CONGRESS CONTROL NUMBER |
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| LC control number |
2010038460 |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
9781439813126 (hardback) |
| 040 ## - CATALOGING SOURCE |
|---|
| Original cataloging agency |
DLC |
| Transcribing agency |
DLC |
| Modifying agency |
DLC |
| 042 ## - AUTHENTICATION CODE |
|---|
| Authentication code |
pcc |
| 050 00 - LIBRARY OF CONGRESS CALL NUMBER |
|---|
| Classification number |
QD77 |
| Item number |
.L47 2011 |
| 082 00 - DEWEY DECIMAL CLASSIFICATION NUMBER |
|---|
| Classification number |
543.028/4 |
| Edition number |
22 |
| 084 ## - OTHER CLASSIFICATION NUMBER |
|---|
| Classification number |
SCI013060 |
| Number source |
bisacsh |
| 100 1# - MAIN ENTRY--PERSONAL NAME |
|---|
| Personal name |
Lerner, Leonid. |
| 245 10 - TITLE STATEMENT |
|---|
| Title |
Small-scale synthesis of laboratory reagents with reaction modeling / |
| Statement of responsibility, etc. |
Leonid Lerner. |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. |
|---|
| Place of publication, distribution, etc. |
Boca Raton : |
| Name of publisher, distributor, etc. |
CRC Press, |
| Date of publication, distribution, etc. |
c2011. |
| 300 ## - PHYSICAL DESCRIPTION |
|---|
| Extent |
xv, 217 p. : |
| Other physical details |
ill. ; |
| Dimensions |
24 cm. |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
|---|
| Bibliography, etc. note |
Includes bibliographical references and index. |
| 520 ## - SUMMARY, ETC. |
|---|
| Summary, etc. |
"The in-lab preparation of some chemical reagents provides a number of advantages over purchasing commercially-prepared samples. This volume contains a detailed description of methods for the rapid and reliable synthesis of many useful reagants that are otherwise difficult to obtain. It provides spectroscopic analyses of products, presents the thermodynamic/kinetic data of reactions, and offers a thorough analysis of the purity of the final products. Enhanced by useful diagrams and photographs, this text is a valuable reference for researchers in small or remote laboratories"-- |
| Assigning source |
Provided by publisher. |
| 520 ## - SUMMARY, ETC. |
|---|
| Summary, etc. |
"When working in a small chemical laboratory attached to a non-chemistry specific project one is frequently asked to solve problems which occur in the main project. Usually one can think of several solutions and experimental testing is required to choose between the different approaches, or indeed to find an approach that works. These often require the use of small amounts of chemicals which the laboratory does not stock. Obtaining these chemicals from commercial suppliers in a suitable timeframe sometimes poses problems. This is particularly the case in isolated regions such as Australasia, when the supplier has no local stocks of hazardous substances and they have to be brought in from overseas, something which can introduce delays from several weeks to six months or more. Since there is no certainty that the substance whose acquisition is introducing the delay will form part of the ultimate solution, this delay is particularly objectionable. The primary aim of this book is therefore to provide reliable laboratory syntheses of the most common reagents whose acquisition can introduce delays due to their hazardous nature. It is apparent that there is little point in replacing delays in reagent purchase with uncertainties in their synthesis, hence the preparations presented in this book were chosen with the following criteria in mind: short duration, availability of apparatus, high yield, and high purity of the product. It was also considered necessary for the syntheses to be described in greater detail than is normally provided in the literature, since I have frequently found that omission of apparently small details can subsequently waste much time"-- |
| Assigning source |
Provided by publisher. |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name entry element |
Chemical tests and reagents |
| General subdivision |
Synthesis. |
| 650 #7 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name entry element |
SCIENCE / Chemistry / Industrial & Technical |
| Source of heading or term |
bisacsh. |
| 906 ## - LOCAL DATA ELEMENT F, LDF (RLIN) |
|---|
| a |
7 |
| b |
cbc |
| c |
orignew |
| d |
1 |
| e |
ecip |
| f |
20 |
| g |
y-gencatlg |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
|---|
| Source of classification or shelving scheme |
Library of Congress Classification |
| Koha item type |
Books |
